Abstract: A method of manufacturing electronics using a nanoparticle ink printing method includes: synthesizing a phase change material (PCM) ink composition using hot injection to develop nanoparticles of the PCM; suspending the nanoparticles with a solvent; and printing a reconfigurable component using the PCM ink composition in additive manufacturing. Electronics includes: a substrate layer; an insulator layer printed on top of the substrate layer; a heater layer printed on top of the insulator layer; a barrier layer printed on top of one or more of the insulator layer and the heater layer; a phase change material (PCM) printed on top of the barrier layer; a connectivity layer printed on top of the PCM; and a passivation layer printed on top of one or more of the PCM and the connectivity layer.

Abstract: The present invention relates to a one-shell aminoplast core-shell microcapsule stabilized by a polyisocyanate. It also provides a method for stabilizing aminoplast microcapsules in liquid aqueous surfactant-rich consumer products.

Abstract: A method is disclosed for synthesis of nanoparticles of metal selenide, metal selenide alloys, metal chalcogenide comprising at least selenium or metal chalcogenide alloys comprising at least selenium. The method comprises obtaining a heterogeneous dispersion of powder at least selenium in a first solvent at a first temperature, the first temperature being such that the heterogeneous dispersion comprises at least a fraction of undissolved powder in the solvent. The method also comprises introducing the heterogeneous dispersion into a second solvent containing a metal cation precursor, the second solvent being at a second temperature higher than said first temperature allowing, upon introduction of the heterogeneous dispersion, dissolution of at least the fraction of the power resulting in nucleation of the nanoparticles. The method results in efficient and easy production of nanoparticles.

Abstract: The present invention teaches microcapsule particles comprising an oil soluble or dispersible core material; and a wall material at least partially surrounding the core material, the microcapsule wall material consisting of the reaction product of a first composition in the presence of a second composition; the first composition comprising a water phase: the water phase comprising a water soluble or dispersible initiator having at least one —COOH or amine functional group and a nonionic emulsifier, the emulsifier comprising a water soluble or dispersible material at a pH from 4 to 12, the water soluble or dispersible initiator is selected from initiators having a C—N?N—C type structure and of formulas I, II or III (set forth in the specification) having amine or carboxyl functionality. The second composition comprises an oil phase.

Abstract: The present invention relates to polymer coated metal powders, such as metal powders used in the formation of solder alloys and pastes. The metal powders are coated with curable compositions of cyanoacrylates. The present invention relates to polymer coated metal powders, such as metal powders used in the formation of solder alloys and pastes. The metal powders are coated with curable compositions of cyanoacrylates, and once cured the coating on the metal powder is a cyanoacrylate polymer.

Abstract: A process of forming a population of microcapsules is described comprising a solid hydrophilic core material and a wall material at least partially surrounding the core material. The microcapsule population is formed by providing an anionic, or optionally a cationic, solid hydrophilic core material; providing an oil continuous phase which is low boiling and preferably nonflammable, the oil continuous phase comprising one or more esters with chain length up to about 18 carbons. A mixture is formed by dispersing the solid hydrophilic material in the oil continuous phase. Either an oil soluble or dispersible amine acrylate or methacrylate, along with acid, or alternatively acid acrylate or methacrylate along with base is added. A multifunctional acrylate or methacrylate monomer or oligomer is provided and an initiator. Optionally a surfactant is also added to form the mixture.

Abstract: The invention relates to nanoparticles having a core that is fully or partially formed by at least one UV-absorbing organic compound in crystallized form and coated with an outer layer formed by at least one hydrophilic polymer, said UV-absorbing organic compound(s) and hydrophilic polymer(s) being associated in a weight ratio of organic compound(s) to hydrophilic polymer(s) varying between 0.2 and 0.4.

Abstract: A W/O emulsion is produced from an aqueous solution containing a substance to be entrapped in a vesicle in a dissolved or suspended state and an oil phase containing an emulsifier; subsequently, the W/O emulsion is cooled to a temperature at which the aqueous solution of the W/O emulsion becomes a frozen particle and the oil phase maintains a liquid state, and the oil phase is removed; thereafter, an oil phase containing a vesicle constituent lipid is added to the frozen particle, and the obtained mixture is then stirred, so as to substitute the emulsifier on the surface of the frozen particle with the vesicle constituent lipid; and thereafter, an external Water phase is added to the frozen particle coated with a lipid membrane, so as to hydrate the lipid membrane by the external water phase. This process achieves a high entrapment yield of a desired substance while controlling desired physical properties such as particle diameter.

Abstract: Methods of making and compositions of dense sintered ceramic nano- and micro-composite materials that are highly stable in a variety of conditions and exhibit superior toughness and strength. Liquid feed flame spray pyrolysis techniques form a plurality of nanoparticles (e.g., powder), each having a core region including a first metal oxide composition comprising Ce and/or Zr or other metals and a shell region including a second metal oxide composition comprising Al or other metals. In certain aspects, the core region comprises a partially stabilized tetragonal ZrO2 and the shell region comprises an ?-Al2O3 phase. The average actual density of the ceramic after sintering is greater than 50% and up to or exceeding 90% of a theoretical density of the ceramic.

Abstract: The present invention deals with an alternative interfacial polymerization process of microencapsulation, microcapsule's produced thereof, microencapsulated agrochemicals, pharmaceuticals, catalysts and phase transfer materials, and formulations thereof, by means of microcapsules and starting materials with much lower toxicological profile than customary microencapsulation materials, and with the participation of acetylene carbamide derivatives in the final structure of the microcapsules' wall.

Abstract: A process for preparing a polymer latex comprising encapsulated pigment particles, said process comprising the steps of: a) Providing a first dispersion comprising water, at least one surfactant and at least one particulate, inorganic pigment of which the particles have a mean diameter of from 200 nm to 10 ?m; b) Providing a second dispersion comprising water, a dispersant, a hydrophobe and at least two polymerizable monomers, of which monomers at least one is an acrylic monomer; c) Independently homogenizing the first and/or second dispersions; d) Mixing said first and second dispersions and homogenizing said mixture until the particles of pigment are encapsulated by monomer droplets; and e) Initiating polymerization of the monomers. In an embodiment, the at least two polymerizable monomers comprise at least one acrylic monomer and at least one monomer being vinyl acetate, styrene or another non-acrylic monomer comprising a polymerizable double bond.

Abstract: Methods for preparing microparticles having reduced residual solvent levels. Microparticles are contacted with a non-aqueous washing system to reduce the level of residual solvent in the microparticles. Preferred non-aqueous washing systems include 100% ethanol and a blend of ethanol and heptane. A solvent blend of a hardening solvent and a washing solvent can be used to harden and wash microparticles in a single step, thereby eliminating the need for a post-hardening wash step.

Abstract: This invention is directed to a process for making solid, typically particulate, water-swellable material comprising coated water-swellable, preferably hydrogel-forming polymers, which are coated with a coating agent, which is such that it does not rupture when the polymers swell in a liquid, e.g., water or saline water. Hereto, the coating agent is extensible in wet state and comprises thereto a wet-extensible material that has a tensile stress at break in the wet state of at least 1 MPa. Typically, the coating agent comprises thereto an elastomeric polymeric material. The invention also relates to solid (particulate) water-swellable material obtainable by the process of the invention.

Abstract: A hydrophobic granular play material comprised of a multitude of engineered particle structures. The particle structures have an average maximum diameter of less than three millimeters. Each particle structure has an inner core of first material that is coated with a hydrophobic composition. The inner core can be particles of natural sand, plastic, or polyfoam. The inner core is enveloped in a composition of a cured elastomeric gel. The gel is hydrophobic. However, the elastomeric gel does exhibit adhesion to itself. Consequently, the particles coated in the elastomeric gel repel water but lightly adhere to each other when compressed together. The particle structures of the play material can therefore be compressed into shapes in the same manner as natural wet sand.

Abstract: The present invention relates to polymer coated metal powders, such as metal powders used in the formation of solder alloys and pastes. The metal powders are coated with curable compositions of cyanoacrylates. The present invention relates to polymer coated metal powders, such as metal powders used in the formation of solder alloys and pastes. The metal powders are coated with curable compositions of cyanoacrylates, and once cured the coating on the metal powder is a cyanoacrylate polymer.

Abstract: A process for producing superhydrophobic powders comprising silica as the main component and the surface of the powders have a contact angle with water of 150° or larger; and a structure having a superhydrophobic surface comprising the powders. The process comprised: introducing hydrophobic groups into the silica present in the surface of aggregates of organic/inorganic composite nanofibers obtained by combining a polymer, which is an organic substance, with silica, which is an inorganic substance, on the order of nanometer or into the silica obtained by calcining the organic/inorganic composite nanofibers and removing the polymer there from; and thereby making powders composed of the aggregates superhydrophobic. Also provided is a superhydrophobic powders obtained by the process. The structure having a superhydrophobic surface is obtained by fixing the superhydrophobic powders to a surface of a solid substrate.

Abstract: The method describes a novel production method for coated particles made of rubber granules, the coating, the particles thus coated, and the use of the coated particles.

Abstract: Composite particles comprised of an optical agent(s) entrapped in a non-porous microparticle of polyorganosilsesquioxane to yield discrete microparticles, are provided. The optical agent is fully encapsulated in the interior of the silsesquioxane particle to impart optical properties that include absorption and emission in the ultraviolet and visible spectrum respectively, without otherwise interfering with the surface chemistry or surface properties of the particle. The use of these novel microparticles in a cosmetic or pharmaceutical composition provides a change in the optical appearance of the skin by either changing the apparent tone or hue, making the skin appear lighter, softer, or by photoluminescent brightening and/or by novel color sculpting under various light conditions.

Abstract: Methods for preparing microparticles having reduced residual solvent levels. Microparticles are contacted with a non-aqueous washing system to reduce the level of residual solvent in the microparticles. Preferred non-aqueous washing systems include 100% ethanol and a blend of ethanol and heptane. A solvent blend of a hardening solvent and a washing solvent can be used to harden and wash microparticles in a single step, thereby eliminating the need for a post-hardening wash step.

Abstract: A composition and a method for fabricating microcapsules encapsulating phase-change material by interfacial condensation polymerization are provided. In this composition and method, a surfactant and an organic solvent are not needed.

Abstract: A method for the production of a robust, chemically stable, crystalline, passivated nanoparticle and composition containing the same, that emit light with high efficiencies and size-tunable and excitation energy tunable color. The methods include the thermal degradation of a precursor molecule in the presence of a capping agent at high temperature and elevated pressure. A particular composition prepared by the methods is a passivated silicon nanoparticle composition displaying discrete optical transitions.

Abstract: The present invention relates to a method for preparing an injectable composition of microparticles for the sustained release of a biologically active agent. The microparticles include a biocompatible polymer and a biologically active agent. The invention provides an improved process for the preparation of microparticles, wherein the physical characteristics of the microparticles, for example, the morphology, density and size, are independent of the process used to prepare the initially formed polymer/drug matrix. The method includes the steps of (a) providing a polymer/biologically active agent matrix; (b) compressing the polymer/biologically active agent matrix, thereby forming a compressed matrix; and (c) fragmenting the compressed matrix, thereby forming an injectable microparticle composition. The polymer/drug matrix can be provided by any suitable method.

Abstract: Algae-resistant roofing granules include inert base particles with an exterior coating including high-surface area silver as a biocide.

Abstract: Methods for preparing microparticles having reduced residual solvent levels. Microparticles are contacted with a non-aqueous washing system to reduce the level of residual solvent in the microparticles. Preferred non-aqueous washing systems include 100% ethanol and a blend of ethanol and heptane. A solvent blend of a hardening solvent and a washing solvent can be used to harden and wash microparticles in a single step, thereby eliminating the need for a post-hardening wash step.

Abstract: The invention is directed to a method for reducing the chemical activity and photo activity of titanium dioxide nanoparticles comprising adding a densifying agent, such as citric acid, to an aqueous slurry of the titanium dioxide nanoparticles; treating the aqueous slurry with a source of silica, such as a solution of sodium silicate, to form silica treated titanium dioxide nanoparticles; treating the silica treated titanium dioxide nanoparticles with a source of alumina, such as a solution of sodium aluminate, to form silica and alumina treated titanium dioxide nanoparticles. The titanium dioxide nanoparticles described herein are useful in cosmetic, coating and polymer compositions.

Abstract: A stabilized emulsion is employed to produce shelf stable, controlled release, discrete, solid particles or pellets which contain an encapsulated and/or embedded component, such as a readily oxidizable component, such as omega-3 fatty acids. An oil encapsulant component which contains an active, sensitive encapsulant, dissolved and/or dispersed in an oil is admixed with an aqueous component and a film-forming component to form an emulsion. An antioxidant for prevention of oxidation of the active, sensitive encapsulant, and a film-softening component or plasticizer for the film-forming component may be included in the emulsion. The emulsion is stabilized by subjecting it to homogenization. The pellets are produced by first reducing the water content of the stabilized emulsion so that the film-forming component forms a film around the oil droplets and encapsulates the encapsulant. In embodiments of the invention, the water content of the homogenized emulsion may be reduced by spray-drying to produce a powder.

Abstract: A display device including: a first substrate having a pixel electrode; a second substrate having a common electrode; a microcapsule sandwiched between the first substrate and the second substrate; and a display material changing its optical characteristic in response to an electrical stimulation, the display material being encapsulated in the microcapsule, the microcapsule being selectively disposed on a display area formed by the pixel electrode in between the first substrate and the second substrate, and a background area of one of the first substrate and the second substrate being colored with a background color, the background area serving as a background with respect to the display area.

Abstract: An article of manufacture containing a substrate and a coating, e.g. optical date storage medium is disclosed. The coating characterised in that real component n and imaginary component k of its refractive index are at least 1.70 and not more than 0.016, respectively, its surface roughness, as the Ra value, is less than 20 nm and a scratch resistance of less than or equal to 0.75 ?m scratch depth. Also disclosed is a process for the production of the coated article.

Abstract: Methods for preparing microparticles having reduced residual solvent levels. Microparticles are contacted with a non-aqueous washing system to reduce the level of residual solvent in the microparticles. Preferred non-aqueous washing systems include 100% ethanol and a blend of ethanol and heptane. A solvent blend of a hardening solvent and a washing solvent can be used to harden and wash microparticles in a single step, thereby eliminating the need for a post-hardening wash step.

Abstract: A method of manufacturing a display that includes a first substrate having a pixel electrode, a second substrate having a common electrode, and a microcapsule interposed between the first and second substrates, a display material being encapsulated in the microcapsule, an optical characteristic of the display material changing in response to an electrical stimulus. The method includes: selectively disposing a microcapsule material that includes the microcapsule on a display area formed of the pixel electrode of the first substrate or an area, of the second substrate, corresponding to the display area; drying the microcapsule material; and joining the first substrate to the second substrate after the drying.

Abstract: This invention relates to a water-swellable material comprising water-swellable polymers that are coated with a coating agent that comprises a phase-separating elastomeric material, which allows swelling of the water-swellable polymers, without breakage of the coating. The invention also relates to a process of making specific coated water-swellable polymers using a phase-separating elastomeric material, and materials obtainable by such a process.

Abstract: An improved method for the preparation of a microsphere from an emulsion wherein an organic phase containing an organic solvent having a boiling point lower than that of water and a hardly-water-soluble polymer is emulsified in an aqueous phase by an in-water drying method, which method includes: (1) providing a gas separation membrane; (2) supplying the emulsion to be subjected to in-water drying to one side of the gas separation membrane; and (3) evaporating off the organic solvent contained in the emulsion to the other side of the gas separation membrane, which can remove the organic solvent with high efficiency and can be carried out in a closed system and hence is favorable from an environmental viewpoint.

Abstract: The present invention teaches an improved process for preparing a population of microcapsules having a substantially uniform size distribution, especially useful for manufacture of carbonless paper. The improved process teaches use of membrane material having a pre-selected pore size in the capsule manufacture process. A core material is provided along with a receiving solution for receiving the core material. The receiving solution is a nonsolvent for the core material. The core material is passed under pressure through the membrane into a moving or turbulent receiving solution forming uniform droplets of core material dispersed in the receiving solution. Wall-forming material is added to the receiving solution for coating the core material droplets. The coating on the droplets is polymerized forming microcapsules. This novel process also lends itself to microcapsule formation in a continuous process.

Abstract: A method for the production of a robust, chemically stable, crystalline, passivated nanoparticle and composition containing the same, that emit light with high efficiencies and size-tunable and excitation energy tunable color. The methods include the thermal degradation of a precursor molecule in the presence of a capping agent at high temperature and elevated pressure. A particular composition prepared by the methods is a passivated silicon nanoparticle composition displaying discrete optical transitions.

Abstract: Methods for preparing microparticles having reduced residual solvent levels. Microparticles are contacted with a non-aqueous washing system to reduce the level of residual solvent in the microparticles. Preferred non-aqueous washing systems include 100% ethanol and a blend of ethanol and heptane. A solvent blend of a hardening solvent and a washing solvent can be used to harden and wash microparticles in a single step, thereby eliminating the need for a post-hardening wash step.

Abstract: A coated ferromagnetic particle comprises a ferromagnetic core and a coating. The coating comprises a residue resulting from a thermal treatment of a coating material comprising a polymer selected from the group consisting of polyorganosiloxanes, polyorganosilanes, and mixtures thereof. A composite magnetic article comprises a compacted and annealed article of a desired shape. The composite magnetic article comprises a plurality of coated ferromagnetic articles. Each coated ferromagnetic particle comprises a ferromagnetic core and a coating. The coating comprises a residue resulting from a thermal treatment of a coating material comprising a polymer selected from the group consisting of polyorganosiloxanes, polyorganosilanes, and mixtures thereof.

Abstract: Micro-encapsulated particles of solid material are described and a quasi-continuous method for the production thereof, in particular those with a water-insoluble character or in a hydrophobised form taking into account in particular an ecologically and economically favourable recycling of the used media and the resultant smallest possible amount of waste products, such as waste water, polymer residues inter alia while simultaneously ensuring the coating even of exposed parts of the solid bodies, such as crystal tips, grooves and the like which, due to the hydrodynamic conditions at these points, can only be coated inadequately with standard methods.

Abstract: A particulate composition comprising particles having a core comprising a hydrophobic polymer within a shell, characterised in that the shell comprises a semi-permeable membrane. Particulate composition can be used for making a stable dispersion of particles uniformly distributed throughout a first hydrophobic liquid, wherein the particles comprise a core within a shell and the core comprises a hydrophobic polymer into has been imbibed a second hydrophobic liquid, Compositions can be used to encapsulate active substances and may be used in sustained release mechanisms.

Abstract: A process for producing a MC-type conductive filler includes treating minute metallic particles with a coupling agent, preparing an oil phase of the coupling agent-treated minute metallic particles and a reactive substance A, the reactive substance A directly contacting the metallic particles. Then, an aqueous phase is prepared having a reactive substance B, which is capable of reacting with the reactive substance A, dissolved in water. Thereafter, the oil phase is dispersed in the aqueous phase to form a suspension. In situ reaction of the reactive substances A and B is then caused by applying heat to the suspension or adding a catalyst to the suspension. This forms a coating of a thermosetting insulating resin on the surface of the minute metallic particles. Alternatively, the reactive substance B may not be used.

Abstract: Described is a process for preparing a dispersion of microcapsules by condensing a partially methylated melamine-formaldehyde resin having a molar ratio of melamine:formaldehyde:methanol of from 1:3.0:2.0 to 1:6.0:4.0 in water in which the essentially water-insoluble material forming the capsule core is present in dispersion in the presence of an alkali metal salt of a homopolymer or copolymer of 2-acrylamido-2-methylpropanesulfonic acid as protective colloid at a pH of from 3 to 6.5 by preforming the microcapsules at a temperature of from 20 to 50° C. and then curing the capsule wall of the preformed microcapsules at >50 to 100° C., which comprises adding from 5 to 100% by weight of melamine, based on the melamine-formaldehyde resin, in the course of curing. The microcapsule dispersions are formaldehyde-reduced and of low viscosity.

Abstract: Powders of particles comprising a ceramic core and a coating of ceria deposited thereon provide an economical and effective abrasive for glass polishing formulations.

Abstract: Methods of making and using annealable insulated metal-based powder particles are provided. The insulated metal-based powder particles are formed from metal-based core particles that are coated with an annealable insulating material. The annealable insulating material has at least one inorganic compound and at least one organic polymeric resin. The inorganic compound in the insulating material forms a nonporous insulating layer surrounding the metal-based core particles upon heating. The organic polymeric resin preferably aids in dispersing or binding the inorganic compound to the metal-based core particles prior to annealing. The insulated metal-based powder particles produced can be formed into core components that can be annealed to improve the magnetic performance of the core component. The core components produced are particularly useful under AC operating conditions of 500 Hz or lower.

Abstract: An edible microcapsule comprising a core and a capsule wall, wherein the core is an edible hydrophobic substance, the capsule wall is formed by salting-out of a combination of a protein and an edible salt, and transglutaminase is used as a crosslinking agent for hardening (solidifying) the capsule wall, and a food containing the edible microcapsule.

Abstract: The present invention relates to colorant compositions containing neonanoplasts. The colorant compositions exhibit improved color brightness and brilliance due to the incorporation of one or more colorants in the neonanoplasts. The colorant compositions may be printed onto virtually any substrate. The colorant compositions of the present invention have particular utility in the area of printed textiles.

Abstract: An edible microcapsule comprising a core and a capsule wall, wherein the core is an edible hydrophobic substance, the capsule wall is formed by salting-out of a combination of a protein and an edible salt, and transglutaminase is used as a crosslinking agent for hardening (solidifying) the capsule wall, and a food containing the edible microcapsule.

Abstract: A particle resistant to storage of at least one first and at least one second component, wherein said second component of at least one crosslinkable polymer as a shell at least partially envelops and/or encloses said first component as a core and said first component has at least one ascertainable property, obtainable by reacting said first component with the crosslinkable polymer and subsequently reacting the formed product with a crosslinking agent such that the first component with resistance to storage remains within the second component.

Abstract: Processes for making microparticles, preferably containing an active agent, are provided. In a preferred embodiment, the process involves preparing (1) a dispersed phase containing an agent in a solution of polymer and a first solvent; (2) a continuous phase containing a surfactant, and a second solvent that is totally or partially immiscible with the first solvent; and (3) an extraction phase that is a nonsolvent for the polymer, a solvent for the continuous phase components, and a solvent for the first solvent, wherein the first solvent has solubility in the extraction phase of between about 0.1% and 25% by weight. Then, the dispersed phase and the continuous phase are mixed to form an emulsion, and the emulsion is then briefly mixed with a suitable quantity of extraction phase to induce skin formation at the interface of the dispersed and continuous phases. Remaining solvent is removed by an evaporation process step.

Abstract: A process for producing a MC-type conductive filler includes treating minute metallic particles with a coupling agent, preparing an oil phase of the coupling agent-treated minute metallic particles and a reactive substance A, the reactive substance A directly contacting the metallic particles. Then, an aqueous phase is prepared having a reactive substance B, which is capable of reacting with the reactive substance A, dissolved in water. Thereafter, the oil phase is dispersed in the aqueous phase to form a suspension. In situ reaction of the reactive substances A and B is then caused by applying heat to the suspension or adding a catalyst to the suspension. This forms a coating of a thermosetting insulating resin on the surface of the minute metallic particles. Alternatively, the reactive substance B may not be used.

Abstract: A method of coating a liquid or solid particulate core involves dropping or suspending the particulate core in an atmosphere and then applying a liquid coating while the particulate core is dropped or suspended, the applying of the liquid coating being done by either (a) spraying the liquid coating onto the particulate core with an ink jet or (b) moving the particulate core through a fog of the liquid coating.

Abstract: A particle resistant to storage of at least one first and at least one second component, wherein